论文标题

用于中子大分子晶体学应用的GD-GEM探测器设计的演示

Demonstration of Gd-GEM detector design for neutron macromolecular crystallography applications

论文作者

Pfeiffer, D., Brunbauer, F., Hall-Wilton, R., Lupberger, M., Marko, M., Muller, H., Oksanen, E., Oliveri, E., Ropelewski, L., Rusu, A., Samarati, J., Scharenberg, L., van Stenis, M., Thuiner, P., Veenhof, R.

论文摘要

瑞典隆德的欧洲散布来源(ESS)将成为世界上最强大的热中子来源。 ESS的大分子衍射仪(NMX)需要三个51.2 x 51.2〜cm $^{2} $检测器,具有合理的检测效率,次-MM空间分辨率,窄点扩散功能(PSF)和良好的时间分辨率。这项工作介绍了NMX检测器原型的改进版本,该原型由带有天然GD转换器的三个GEM探测器和低材料预算读数组成。该检测器在布达佩斯中子中心(BNC)的中子反应堆和格勒诺布尔研究所的D16仪器上成功测试。布达佩斯中用镉和gadolinium面具的测量结果表明,检测器的点扩散功能缺乏可能阻碍衍射点强度测量的长尾巴。在ILL的D16仪器上,在D16氦-3检测器和GD-GEM中测量了2-磷酸三磷酸异构酶(PGA)抑制剂的衍射点。与氦3检测器相比,两个检测器之间的比较在两个检测器中都显示出相似的点扩散功能,而预期效率比。因此,这两种测量值都很好地表明了GD-GEM探测器适合ESS的NMX仪器的要求。

The European Spallation Source (ESS) in Lund, Sweden will become the world's most powerful thermal neutron source. The Macromolecular Diffractometer (NMX) at the ESS requires three 51.2 x 51.2~cm$^{2}$ detectors with reasonable detection efficiency, sub-mm spatial resolution, a narrow point spread function (PSF) and good time resolution. This work presents measurements with the improved version of the NMX detector prototype consisting of a Triple-GEM detector with natural Gd converter and a low material budget readout. The detector was successfully tested at the neutron reactor of the Budapest Neutron Centre (BNC) and at the D16 instrument at the Institut Laue-Langevin (ILL) in Grenoble. The measurements with Cadmium and Gadolinium masks in Budapest demonstrate that the point spread function of the detector lacks long tails that could impede the measurement of diffraction spot intensities. On the D16 instrument at ILL, diffraction spots from Triose phosphate isomerase w/ 2-phosphoglycolate (PGA) inhibitor were measured both in the D16 Helium-3 detector and the Gd-GEM. The comparison between the two detectors show a similar point spread function in both detectors, and the expected efficiency ratio compared to the Helium-3 detector. Both measurements together thus give good indications that the Gd-GEM detector fits the requirements for the NMX instrument at ESS.

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