论文标题

在湍流测量中制造独立式PT纳米线以用作热诊断探针

Fabrication of free-standing Pt nanowires for use as thermal anemometry probes in turbulence measurements

论文作者

Le-The, Hai, Küchler, Christian, Berg, Albert van den, Bodenschatz, Eberhard, Lohse, Detlef, Krug, Dominik

论文摘要

我们报告了一种强大的制造方法,用于对独立的PT纳米线进行构图,以用作小规模湍流测量的热疫脉测定探针。使用电子束光刻,在氧化硅(SI)晶状体的表面上绘制了高纵横比PT纳米线(〜300 nm宽度,〜70 $μ$ m的长度,〜100 nm厚)。将精确的湿蚀刻过程与干蚀刻过程相结合,这些PT纳米线在SI悬臂支持的两个二氧化硅(SIO2)梁之间成功释放了自由释放。此外,固定设备的桥梁的独特设计使设备可以轻轻释放设备而不会损坏PT纳米线。通过将电子束光刻的使用限制为PT纳米线的图案,将总制造时间降至最低,而在其他部分则使用标准光刻。我们证明,在恒定模式下操作时,制造的传感器适用于湍流测量。在SF6大气中,在2 bar的压力和21°C的温度下,在SF6大气中建立了在0.5 m S-1到5 m S-1之间的输出电压和流体速度之间的稳健校准。来自纳米线的传感信号在几个小时的时间内显示出可忽略的漂移。此外,我们确认纳米线能够通过在最高55 m/s的室温速度下在空气中测试空气来承受高动态压力。

We report a robust fabrication method for patterning free-standing Pt nanowires for the use as thermal anemometry probes for small-scale turbulence measurements. Using e-beam lithography, high aspect ratio Pt nanowires (~300 nm width, ~70 $μ$m length, ~100 nm thickness) were patterned on the surface of oxidized silicon (Si) wafers. Combining precise wet etching processes with dry etching processes, these Pt nanowires have been successfully released free-standing between two silicon dioxide (SiO2) beams supported on Si cantilevers. Moreover, the unique design of the bridge holding the device allowed to release the device gently without damaging the Pt nanowires. The total fabrication time was minimized by restricting the use of e-beam lithography to the patterning of the Pt nanowires while standard photolithography was employed for other parts of the devices. We demonstrate that the fabricated sensors are suitable for turbulence measurements when operated in a constant-current mode. A robust calibration between output voltage and fluid velocity was established over the velocity range from 0.5 m s-1 to 5 m s-1 in an SF6 atmosphere at a pressure of 2 bar and a temperature of 21°C. The sensing signal from the nanowires showed negligible drift over a period of several hours. Moreover, we confirmed that the nanowires are able to withstand high dynamic pressures by testing them in air at room temperature velocities up to 55 m/s.

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